4OZN
GlnK2 from Haloferax mediterranei complexed with ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-08 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.8726 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 110.717, 110.717, 76.949 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.980 - 2.600 |
R-factor | 0.21804 |
Rwork | 0.217 |
R-free | 0.24348 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.139 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 47.900 |
High resolution limit [Å] | 1.440 |
Number of reflections | 17092 |
<I/σ(I)> | 8.2 |
Completeness [%] | 100.0 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 0.5 M Lithium sulphate, 15% PEG 8000 |