4OZK
Crystal structure of Laterosporulin, a broad spectrum leaderless bacteriocin produced by Brevibacillus laterosporus strain GI-9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2012-12-12 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 3 2 |
Unit cell lengths | 65.000, 65.000, 65.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.069 - 2.038 |
R-factor | 0.1976 |
Rwork | 0.196 |
R-free | 0.22740 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.049 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.20) |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.000 | 45.962 | 2.140 |
High resolution limit [Å] | 2.038 | 6.430 | 2.030 |
Rmerge | 0.037 | 0.436 | |
Rmeas | 0.122 | ||
Rpim | 0.037 | 0.015 | 0.146 |
Total number of observations | 34934 | 1176 | 4499 |
Number of reflections | 3319 | ||
<I/σ(I)> | 17 | 35 | 5.3 |
Completeness [%] | 98.9 | 98.7 | 92.8 |
Redundancy | 10.5 | 8.5 | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.1 M TRIS pH 8.5, 3M NaCl |