4OZJ
GlnK2 from Haloferax mediterranei complexed with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-09-22 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | H 3 2 |
Unit cell lengths | 89.185, 89.185, 96.349 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 60.260 - 1.450 |
R-factor | 0.17423 |
Rwork | 0.173 |
R-free | 0.18987 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.425 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.260 |
High resolution limit [Å] | 1.320 |
Number of reflections | 25401 |
<I/σ(I)> | 21.9 |
Completeness [%] | 96.8 |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 294 | 2M ammonium sulphate, 0.1 M NaCitrate, 0.2 M Na/K Tartrate |