4OZJ
GlnK2 from Haloferax mediterranei complexed with ADP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-09-22 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 89.185, 89.185, 96.349 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 60.260 - 1.450 |
| R-factor | 0.17423 |
| Rwork | 0.173 |
| R-free | 0.18987 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.425 |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 60.260 |
| High resolution limit [Å] | 1.320 |
| Number of reflections | 25401 |
| <I/σ(I)> | 21.9 |
| Completeness [%] | 96.8 |
| Redundancy | 7.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 294 | 2M ammonium sulphate, 0.1 M NaCitrate, 0.2 M Na/K Tartrate |
