4OZI

S2 protein complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2013-07-28
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.95370
Spacegroup name	C 1 2 1
Unit cell lengths	233.027, 142.239, 101.090
Unit cell angles	90.00, 109.79, 90.00

Refinement procedure

Resolution	46.850 - 3.200
R-factor	0.2141
Rwork	0.212
R-free	0.24340
RMSD bond length	0.009
RMSD bond angle	0.970
Refinement software	BUSTER (2.10.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	46.850
High resolution limit [Å]	3.200
Rmerge	0.159
Number of reflections	49219
<I/σ(I)>	4.24
Completeness [%]	96.1
Redundancy	1.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293.15	Mother liquor: 0.15- 0.25M CaOAc, 0.1 M Tris/HCl, 12-18% PEG3350, Additives: 2-3 mM reduced and oxidised Glutathione