4OYV
Crystal structure of MltF from Pseudomonas aeruginosa complexed with leucine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2012-03-06 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.542 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 53.616, 82.495, 89.842 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.200 - 2.310 |
R-factor | 0.2314 |
Rwork | 0.228 |
R-free | 0.30400 |
RMSD bond length | 0.013 |
RMSD bond angle | 1.595 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.20) |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.040 | 2.430 |
High resolution limit [Å] | 2.310 | 2.310 |
Rmerge | 0.092 | 0.175 |
Rmeas | 0.110 | |
Rpim | 0.059 | |
Total number of observations | 65955 | |
Number of reflections | 17631 | |
<I/σ(I)> | 7 | 4.9 |
Completeness [%] | 97.5 | 94.7 |
Redundancy | 3.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 0.1 M Tris pH 8.0, 0.2 M MgCl2, 20% (W/V) PEG 8000. |