4OYH

Structure of Bacillus subtilis MobB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-11-10
Detector	ADSC QUANTUM 270
Wavelength(s)	1.0
Spacegroup name	C 1 2 1
Unit cell lengths	225.528, 42.107, 93.620
Unit cell angles	90.00, 100.99, 90.00

Refinement procedure

Resolution	29.271 - 2.409
R-factor	0.2152
Rwork	0.210
R-free	0.30340
RMSD bond length	0.014
RMSD bond angle	1.559
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.400
Number of reflections	33530
<I/σ(I)>	9
Completeness [%]	98.8
Redundancy	25

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	25% PEG3350 0.4M Ammonium sulfate