4OYF
Crystal structure of GLTPH R397A IN Sodium-bound state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9700 |
Spacegroup name | P 31 |
Unit cell lengths | 110.579, 110.579, 306.923 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 12.000 - 3.410 |
R-factor | 0.28474 |
Rwork | 0.284 |
R-free | 0.29348 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.468 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 12.000 |
High resolution limit [Å] | 3.410 |
Number of reflections | 48366 |
<I/σ(I)> | 13.8 |
Completeness [%] | 87.3 |
Redundancy | 11.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG400 sodium chloride citrate/tris |