4OY5
0.89 Angstrom resolution crystal structure of (Gly-Pro-Hyp)10
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-13 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.7293 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 13.860, 26.150, 19.880 |
Unit cell angles | 90.00, 105.43, 90.00 |
Refinement procedure
Resolution | 19.160 - 0.890 |
R-factor | 0.06773 |
Rwork | 0.067 |
R-free | 0.07732 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.047 |
RMSD bond angle | 4.406 |
Phasing software | SHELXDE (2013/1) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.190 | 0.910 |
High resolution limit [Å] | 0.890 | 0.890 |
Number of reflections | 10270 | |
<I/σ(I)> | 54.7 | 25.4 |
Completeness [%] | 96.5 | 93.9 |
Redundancy | 7.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 22% PEG400, 5% acetic acid |