4OXV
Crystal structure of MltF from Pseudomonas aeruginosa complexed with valine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2012-03-01 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.542 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.881, 80.671, 89.219 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.950 - 2.200 |
R-factor | 0.1792 |
Rwork | 0.176 |
R-free | 0.24410 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.629 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.880 | 2.430 |
High resolution limit [Å] | 2.200 | 2.310 |
Rmerge | 0.510 | |
Number of reflections | 19799 | |
<I/σ(I)> | 6.9 | 2.6 |
Completeness [%] | 99.2 | 94.7 |
Redundancy | 4.1 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 277 | 0.1 M Tris pH 8.0, 0.2 M MgCl2, 20% (W/V) PEG 8000. |