4OXC
Crystal structure of XIAP BIR1 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.630, 72.390, 69.870 |
Unit cell angles | 90.00, 95.69, 90.00 |
Refinement procedure
Resolution | 50.190 - 2.900 |
R-factor | 0.18 |
Rwork | 0.176 |
R-free | 0.25100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.142 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.400 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.121 | 0.615 |
Number of reflections | 8085 | |
<I/σ(I)> | 7.1 | |
Completeness [%] | 99.2 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 8.5 | 293 | PEG 4000, Sodium Acetate |