4OWT
Structural basis of SOSS1 complex assembly
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9793 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 116.809, 116.809, 109.832 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.900 - 2.000 |
R-factor | 0.173 |
Rwork | 0.172 |
R-free | 0.19500 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.993 |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8.1_1168)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 58840 |
<I/σ(I)> | 9.9 |
Completeness [%] | 100.0 |
Redundancy | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 21% PEG2000 MME, 0.1M MES pH6.0, 0.05M sodium chloride |