4OWI
peptide structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-03-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97935 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 30.480, 29.390, 32.700 |
Unit cell angles | 90.00, 98.25, 90.00 |
Refinement procedure
Resolution | 30.165 - 1.202 |
R-factor | 0.1632 |
Rwork | 0.162 |
R-free | 0.19470 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.157 |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.165 |
High resolution limit [Å] | 1.200 |
Number of reflections | 17562 |
<I/σ(I)> | 59.73 |
Completeness [%] | 97.5 |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291.15 | ethanol |