4OVO

REFINED X-RAY CRYSTAL STRUCTURES OF THE REACTIVE SITE MODIFIED OVOMUCOID INHIBITOR THIRD DOMAINS FROM SILVER PHEASANT (OMSVP3(ASTERISK)) AND FROM JAPANESE QUAIL (OMJPQ3(ASTERISK))

Experimental procedure

Spacegroup name	I 4 2 2
Unit cell lengths	56.600, 56.600, 76.200
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 * - 2.500
R-factor	0.185 *
Rwork	0.185
RMSD bond length	0.011
RMSD bond angle	2.320
Refinement software	EREF

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.094 *
Total number of observations	5813 *
Number of reflections	1947 *
Completeness [%]	82.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6 *	20 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	1.45 (M)
2	1	drop	protein	15 (mg/ml)