4ORL
Crystal structure of a DUF4783 family protein (BACOVA_04304) from Bacteroides ovatus ATCC 8483 at 1.40 A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-01-23 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 2 |
Unit cell lengths | 47.635, 103.233, 43.234 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.894 - 1.400 |
R-factor | 0.1832 |
Rwork | 0.182 |
R-free | 0.20850 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.126 |
Data reduction software | XDS |
Data scaling software | XSCALE (July 4, 2012) |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 27.894 | 27.894 | 1.450 |
High resolution limit [Å] | 1.400 | 3.010 | 1.400 |
Rmerge | 0.023 | 0.013 | 0.393 |
Number of reflections | 21177 | 3843 | 3848 |
<I/σ(I)> | 18.78 | 54.6 | 2.3 |
Completeness [%] | 96.7 | 93.5 | 95.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.2 | 277 | 40.00% polyethylene glycol 600, 0.1M phosphate-citrate pH 4.2, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |