4OQJ
Streptomcyes albus JA3453 oxazolomycin ketosynthase domain OzmQ KS1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-07-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9794 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 93.512, 129.455, 85.088 |
Unit cell angles | 90.00, 98.64, 90.00 |
Refinement procedure
Resolution | 30.205 - 1.904 |
R-factor | 0.1516 |
Rwork | 0.150 |
R-free | 0.17870 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.050 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | HKL-3000 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.044 | |
Number of reflections | 75965 | |
<I/σ(I)> | 26 | |
Completeness [%] | 98.3 | 88.1 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.2 | 289 | 1.0 M NaH2PO4/K2HPO4, pH 8.2, VAPOR DIFFUSION, HANGING DROP, temperature 289K |