4OQ1
Structure of the Streptococcal ancillary pilin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97923 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.580, 65.760, 60.420 |
Unit cell angles | 90.00, 110.97, 90.00 |
Refinement procedure
Resolution | 34.630 - 1.850 |
R-factor | 0.1882 |
Rwork | 0.186 |
R-free | 0.23692 |
Structure solution method | SAD |
RMSD bond length | 0.022 |
RMSD bond angle | 2.000 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | PHENIX (refine) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.630 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.149 | 0.502 |
Number of reflections | 26430 | |
<I/σ(I)> | 7.1 | 3 |
Completeness [%] | 80.0 | 96.1 |
Redundancy | 6.9 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1 M Bis-Tris, 28% w/v PEG2000, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 0.1 M Bis-Tris, 28% w/v PEG2000, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |