4OLE
Crystal structure of a neighbor of BRCA1 gene 1 (NBR1) from Homo sapiens at 2.52 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-27 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97891,0.97949,0.91837 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 111.457, 111.457, 230.607 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.720 - 2.520 |
R-factor | 0.1737 |
Rwork | 0.173 |
R-free | 0.18820 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.060 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | BUSTER-TNT (2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 48.720 | 48.720 | 2.610 |
High resolution limit [Å] | 2.520 | 5.400 | 2.520 |
Rmerge | 0.122 | 0.056 | 1.222 |
Number of reflections | 50067 | 5435 | 4894 |
<I/σ(I)> | 15.26 | 34 | 2.09 |
Completeness [%] | 99.9 | 99.3 | 99.9 |
Redundancy | 8.76 | 9.01 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.33 | 277 | 2.35M ammonium sulfate, 0.1M TRIS pH 8.33, 0.01M Adenosine-5'-triphosphate disodium salt hydrate, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 277K |