4OIH
Importin Alpha in Complex with the Bipartite NLS of Prp20
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954946 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.910, 89.920, 99.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.370 - 2.100 |
R-factor | 0.16941 |
Rwork | 0.168 |
R-free | 0.20125 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ul1 |
RMSD bond length | 0.022 |
RMSD bond angle | 2.081 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.370 | 2.154 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 53834 | |
Completeness [%] | 99.8 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 296.15 | 500mM sodium citrate, 10mM DTT, pH 6.0-8.0, VAPOR DIFFUSION, HANGING DROP, temperature 296.15K |