4OI6
Crystal structure analysis of nickel-bound form SCO4226 from Streptomyces coelicolor A3(2)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-11-13 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 28.330, 67.140, 35.090 |
Unit cell angles | 90.00, 94.98, 90.00 |
Refinement procedure
Resolution | 17.536 - 2.040 |
R-factor | 0.1729 |
Rwork | 0.171 |
R-free | 0.21650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.067 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.536 | 2.140 |
High resolution limit [Å] | 2.040 | 2.040 |
Number of reflections | 8364 | |
Completeness [%] | 98.3 | 88.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 289 | 0.8 M sodium citrate dihydrate, pH 6.5 and 0.8 M NiSO4, VAPOR DIFFUSION, HANGING DROP, temperature 289K |