4OHV
C. Elegans Clp1 bound to AMP-PNP, and Mg2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-03-29 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 31 |
Unit cell lengths | 100.720, 100.720, 40.380 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 87.230 - 2.300 |
R-factor | 0.19463 |
Rwork | 0.192 |
R-free | 0.23955 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.312 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | HKL2Map |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 87.230 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 40589 | |
Completeness [%] | 99.7 | 99.5 |
Redundancy | 4.8 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 100 mM Na2HPO4/KH2PO4 200 mM NaCl 15 mM MgCl2 90 mM sarcosine 25% (w/v) PEG 1000, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |