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4OH3

Crystal structure of a nitrate transporter

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2010-10-10
DetectorADSC QUANTUM 315r
Wavelength(s)1.0
Spacegroup nameC 2 2 21
Unit cell lengths84.800, 188.465, 262.848
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution45.909 - 3.250
R-factor0.2384
Rwork0.235
R-free0.30670
Structure solution methodSAD
RMSD bond length0.010
RMSD bond angle1.454
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.8.4_1496))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.260
High resolution limit [Å]3.2503.200
Rmerge0.0700.910
Number of reflections34573
<I/σ(I)>1.21.4
Completeness [%]99.093.5
Redundancy5.94.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.52770.1M sodium acetate 30% PEG300 3% MPD, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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