4OFY
Crystal Structure of the Complex of SYG-1 D1-D2 and SYG-2 D1-D4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-06-05 |
Detector | MARMOSAIC 325 mm CCD |
Wavelength(s) | 1.0088 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 286.786, 116.144, 98.032 |
Unit cell angles | 90.00, 107.62, 90.00 |
Refinement procedure
Resolution | 41.061 - 3.300 |
R-factor | 0.2619 |
Rwork | 0.259 |
R-free | 0.30590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB Entries 4OF3 4ofp |
RMSD bond length | 0.004 |
RMSD bond angle | 0.904 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1593)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.300 |
Number of reflections | 44580 |
<I/σ(I)> | 13.4 |
Completeness [%] | 95.9 |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.4 | 295 | 16% PEG 3,350, 0.2 M Triammonium citrate, 0.1 M MES pH 6.4, VAPOR DIFFUSION, SITTING DROP, temperature 295.0K |