4OFV
Refinement of RAGE-DNA complex in 3S58 without DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Detector technology | CCD |
Detector | MARMOSAIC 300 mm CCD |
Spacegroup name | P 61 |
Unit cell lengths | 77.920, 77.920, 224.387 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.140 - 3.100 |
R-factor | 0.221 |
Rwork | 0.220 |
R-free | 0.24000 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 3S58 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.673 |
Refinement software | PHENIX (1.8.3_1479) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.100 |
Number of reflections | 13817 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.4 | 298 | 12% PEG6000, 0.1 M Tris-HCl, pH 7.4, VAPOR DIFFUSION, HANGING DROP, temperature 298K |