Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-05-04 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97939 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 303.250, 320.730, 667.620 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.999 - 3.502 |
| R-factor | 0.2442 |
| Rwork | 0.243 |
| R-free | 0.29500 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.334 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA (3.3.21) |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 73.112 |
| High resolution limit [Å] | 3.502 |
| Number of reflections | 628863 |
| <I/σ(I)> | 6 |
| Completeness [%] | 99.7 |
| Redundancy | 8.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.1 M HEPES pH 7.0, 0.1 % Jeffamine ED-2001 and 1.1 M sodium malonate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
