Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2009-11-18 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9794, 0.97912 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 103.425, 103.425, 131.951 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 74.110 - 2.097 |
| R-factor | 0.1662 |
| Rwork | 0.165 |
| R-free | 0.19502 |
| Structure solution method | MAD |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.568 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 74.110 | 2.140 |
| High resolution limit [Å] | 2.097 | 2.097 |
| Rmerge | 0.082 | 0.957 |
| Number of reflections | 48245 | |
| <I/σ(I)> | 36.6 | 2.2 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 14.5 | 14 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 289 | 1.0M succinic acid, 0.1M Bis-Tris Propane, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 289.0K |
