4O35
Crystal structure of carbomonoxy murine neuroglobin mutant F106W
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-2 |
Synchrotron site | ESRF |
Beamline | ID23-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-04-08 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.8732 |
Spacegroup name | H 3 2 |
Unit cell lengths | 89.155, 89.155, 108.622 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.183 - 1.800 |
R-factor | 0.192 |
Rwork | 0.188 |
R-free | 0.23360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.515 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.183 | 1.864 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 15481 | |
Completeness [%] | 99.1 | 99.61 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.6M ammonium sulphate, 0.1M MES, 10% dioxane, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |