4NNR
FKBP13-FK506 Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 293 |
Detector technology | AREA DETECTOR |
Collection date | 1993-07-17 |
Detector | UCSD MARK II |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.260, 74.060, 39.240 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 17.300 - 1.980 |
R-factor | 0.159 |
Rwork | 0.159 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.653 |
Data reduction software | SDMS |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 18.000 | 3.380 | 2.130 |
High resolution limit [Å] | 1.980 | 2.690 | 1.980 |
Number of reflections | 13559 | ||
Completeness [%] | 87.0 | 95 | 53 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | VAPOR DIFFUSION, HANGING DROP, pH 7, temperature 298K |