4NNR
FKBP13-FK506 Complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 293 |
| Detector technology | AREA DETECTOR |
| Collection date | 1993-07-17 |
| Detector | UCSD MARK II |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 74.260, 74.060, 39.240 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 17.300 - 1.980 |
| R-factor | 0.159 |
| Rwork | 0.159 |
| R-free | 0.22100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.653 |
| Data reduction software | SDMS |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 18.000 | 3.380 | 2.130 |
| High resolution limit [Å] | 1.980 | 2.690 | 1.980 |
| Number of reflections | 13559 | ||
| Completeness [%] | 87.0 | 95 | 53 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | VAPOR DIFFUSION, HANGING DROP, pH 7, temperature 298K |
