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4NM0

Crystal structure of peptide inhibitor-free GSK-3/Axin complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL11-1
Synchrotron siteSSRL
BeamlineBL11-1
Temperature [K]100
Detector technologyPIXEL
Collection date2013-06-09
DetectorPSI PILATUS 6M
Wavelength(s)1.033
Spacegroup nameP 61 2 2
Unit cell lengths81.303, 81.303, 280.829
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution39.048 - 2.500
R-factor0.1931
Rwork0.191
R-free0.23950
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4nm7
RMSD bond length0.003
RMSD bond angle0.626
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.8.2_1309))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]39.0502.600
High resolution limit [Å]2.5002.500
Rmeas0.1121.8390.017
Rpim0.0360.5760.006
Total number of observations192347217703969
Number of reflections20069
<I/σ(I)>18.41.2
Completeness [%]100.099.9
Redundancy9.69.9
CC(1/2)0.9990.7261.000
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1MICRODIALYSIS7.527710% PEG 35,000, 20mM Tris 7.5, 300mM NaCl, 5% glycerol, 20mM MgCl2, 400uM ATP, and 5mM DTT, MICRODIALYSIS, temperature 277K

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