4NKN
The Crystal Structure of the N-terminal domain of COMMD9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-18 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95370 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 89.690, 79.757, 131.164 |
Unit cell angles | 90.00, 90.61, 90.00 |
Refinement procedure
Resolution | 32.789 - 2.790 |
R-factor | 0.2117 |
Rwork | 0.210 |
R-free | 0.24950 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.396 |
Data reduction software | XDS |
Data scaling software | Aimless (0.1.27) |
Phasing software | PHASER (2.5.3) |
Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 39.460 | 39.460 | 2.940 |
High resolution limit [Å] | 2.790 | 8.810 | 2.790 |
Rmerge | 0.093 | 0.046 | 0.646 |
Total number of observations | 5392 | 23049 | |
Number of reflections | 23054 | ||
<I/σ(I)> | 16 | 42.8 | 3.2 |
Completeness [%] | 98.6 | 99 | 91.6 |
Redundancy | 3.8 | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 291.15 | 20% PEG 3350, 0.2M Mg Nitrate, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 291.15K |