4NJ7
PB1 Domain of AtARF7 - SeMet Derivative
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2013-08-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.979 |
Spacegroup name | H 3 |
Unit cell lengths | 150.936, 150.936, 184.236 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.600 - 3.000 |
R-factor | 0.261 |
Rwork | 0.257 |
R-free | 0.30400 |
Structure solution method | SAD |
RMSD bond length | 0.025 |
RMSD bond angle | 2.048 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.634 | 3.180 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 28097 | |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 20% PEG-3350, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |