4NIJ

X-ray structure of the complex between hen egg white lysozyme and pentachlorocarbonyliridate(III) (30 days)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Collection date	2012-11-04
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	77.042, 77.042, 37.244
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 1.860
R-factor	0.2338
Rwork	0.211
R-free	0.25660
Structure solution method	FOURIER SYNTHESIS
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.800
Rmerge	0.116
Number of reflections	10384
Completeness [%]	95.3
Redundancy	5.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.5	298	Ir(Cl)5CO for 30 days, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K