Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL26B2 |
Synchrotron site | SPring-8 |
Beamline | BL26B2 |
Temperature [K] | 100 |
Wavelength(s) | 0.8 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 50.398, 90.721, 53.370 |
Unit cell angles | 90.00, 102.72, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
R-factor | 0.168 |
Rwork | 0.168 |
Structure solution method | MOLECULAR REPLACEMENT |
Refinement software | SHELX |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.600 |
Number of reflections | 55988 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |