4NEI
Alg17c PL17 Family Alginate Lyase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Detector technology | CCD |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97852 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.530, 126.351, 87.631 |
Unit cell angles | 90.00, 111.51, 90.00 |
Refinement procedure
Resolution | 25.000 - 1.850 |
R-factor | 0.16957 |
Rwork | 0.168 |
R-free | 0.19228 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.015 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHARP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.880 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 144904 | |
Completeness [%] | 98.3 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 290 | 10% PEG 6000, 5% MPD, 100 mM Tris, pH=8.0, VAPOR DIFFUSION, HANGING DROP, temperature 290K |