4NAF
PrcB from Geobacillus kaustophilus, apo structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Detector technology | CCD |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 85.114, 157.840, 38.170 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.435 - 1.900 |
R-factor | 0.2139 |
Rwork | 0.212 |
R-free | 0.24080 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.932 |
Refinement software | PHENIX ((phenix.refine: dev_1422)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 27.435 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.038 |
Number of reflections | 41523 |
Completeness [%] | 99.9 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |