4NAE
PcrB from Geobacillus kaustophilus, with bound G1P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Detector technology | CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 85.350, 157.970, 38.090 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.416 - 2.000 |
R-factor | 0.2043 |
Rwork | 0.202 |
R-free | 0.24280 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.157 |
Refinement software | PHENIX ((phenix.refine: dev_1422)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 29.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.038 |
Number of reflections | 151551 |
Completeness [%] | 80.0 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 19% w/v PEG4000, VAPOR DIFFUSION, HANGING DROP |