4N6Q
Crystal structure of VosA velvet domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 2010-10-13 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 41 2 2 |
Unit cell lengths | 45.400, 45.400, 189.430 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.100 - 1.790 |
R-factor | 0.1851 |
Rwork | 0.183 |
R-free | 0.22030 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.567 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELX |
Refinement software | PHENIX (1.7.2_869) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 32.100 | 8.000 | 1.840 |
High resolution limit [Å] | 1.790 | 5.660 | 1.790 |
Rmerge | 0.036 | 0.024 | 0.286 |
Number of reflections | 19471 | 721 | 2440 |
<I/σ(I)> | 22.17 | 47.47 | 4.64 |
Completeness [%] | 99.2 | 100 | 92 |
Redundancy | 4.01 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 100 mM MES, pH 6.5, 32% PEG 2000 MME, 150 mM KI, VAPOR DIFFUSION, SITTING DROP, temperature 293K |