4N2L

Crystal structure of Protein Arginine Deiminase 2 (Q350A, 10 mM Ca2+)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 21-ID-G
Synchrotron site	APS
Beamline	21-ID-G
Detector technology	CCD
Detector	MARMOSAIC 300 mm CCD
Wavelength(s)	0.9787
Spacegroup name	C 1 2 1
Unit cell lengths	203.380, 51.100, 76.180
Unit cell angles	90.00, 105.60, 90.00

Refinement procedure

Resolution	40.242 - 2.100
R-factor	0.1678
Rwork	0.165
R-free	0.21530
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4n25
RMSD bond length	0.011
RMSD bond angle	1.219
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.7.2_869)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.242
High resolution limit [Å]	2.100	2.100
Number of reflections	44320

Crystallization Conditions

crystal ID	method	pH	temperature	details
1