4N0L
Methanopyrus kandleri Csm3 crystal structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-09-19 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.99999 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 95.753, 101.017, 174.167 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 69.494 - 2.370 |
| R-factor | 0.195 |
| Rwork | 0.194 |
| R-free | 0.21560 |
| Structure solution method | Zn-SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.825 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 69.494 | 2.400 |
| High resolution limit [Å] | 2.370 | 2.370 |
| Number of reflections | 66282 | |
| Completeness [%] | 99.4 | 99.44 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 0.05M MES, 50% MPD, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
