4N0G
Crystal Structure of PYL13-PP2CA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-16 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 3 |
Unit cell lengths | 111.383, 111.383, 70.410 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.790 - 2.382 |
R-factor | 0.2125 |
Rwork | 0.211 |
R-free | 0.24490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rto |
RMSD bond length | 0.009 |
RMSD bond angle | 1.170 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.470 |
High resolution limit [Å] | 2.380 | 2.380 |
Number of reflections | 38995 | |
Completeness [%] | 99.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 100mM MES pH 6.5, 25% PEG600, 150mM Calcium Chloride, 2.7% 2,5-Hexanediol, VAPOR DIFFUSION, HANGING DROP, temperature 291K |