4MXI
ClpP Ser98dhA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-03-16 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 121.590, 121.590, 402.950 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.300 |
R-factor | 0.19741 |
Rwork | 0.196 |
R-free | 0.22075 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v5e |
RMSD bond length | 0.006 |
RMSD bond angle | 0.890 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.400 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.057 | 0.589 |
Number of reflections | 79191 | |
<I/σ(I)> | 23.34 | 4.85 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | 0.1 M Citric acid, 2.0 M (NH4)2SO4, pH 4.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |