Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Detector technology | IMAGE PLATE |
Collection date | 2003-06-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 102.696, 212.399, 198.740 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.228 - 2.400 |
R-factor | 0.1724 |
Rwork | 0.170 |
R-free | 0.21490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1R9E |
RMSD bond length | 0.008 |
RMSD bond angle | 1.065 |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.400 |
Number of reflections | 83283 |
Completeness [%] | 97.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 6.5 | PEG 3350, TRI-AMMONIUM CITRATE, CAPILLARY BATCH, pH 6.5, EVAPORATION |