4MTE
Zinc Uptake Regulator Complexed with Zinc and DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 78 |
Detector technology | CCD |
Collection date | 2011-02-07 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.97872 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 193.324, 80.470, 98.770 |
Unit cell angles | 90.00, 120.15, 90.00 |
Refinement procedure
Resolution | 36.340 - 2.500 |
R-factor | 0.2195 |
Rwork | 0.217 |
R-free | 0.25690 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.953 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHARP |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.400 | 2.610 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.046 | 0.290 |
Number of reflections | 45429 | |
<I/σ(I)> | 19.4 | 5 |
Completeness [%] | 99.8 | 99 |
Redundancy | 4.1 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 277 | 1.5 M Ammonium Sulfate, 0.1 M Citrate, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |