4MT2
COMPARISON OF THE NMR SOLUTION STRUCTURE AND THE X-RAY CRYSTAL STRUCTURE OF RAT METALLOTHIONEIN-2
Replaces: 2MT2Replaces: 1MT2Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 30.900, 30.900, 120.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 2.000 |
Rwork | 0.197 |
RMSD bond length | 0.020 |
RMSD bond angle | 3.500 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * | 22 * | Melis, K.A., (1983) J.Biol.Chem., 258, 6255. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | sodium formate | 1.0 (M) | |
3 | 1 | drop | potassium phosphate | 0.2 (M) | |
4 | 1 | reservoir | sodium formate | 5.0 (M) |