4MH3
Crystal structure of Bovine Mitochondrial Peroxiredoxin III
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-12-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 142.895, 290.885, 81.139 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 102.140 - 2.400 |
R-factor | 0.184 |
Rwork | 0.182 |
R-free | 0.22116 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1zye |
RMSD bond length | 0.012 |
RMSD bond angle | 1.581 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 288.670 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.073 | 0.732 |
Number of reflections | 130007 | |
<I/σ(I)> | 11.3 | 1.8 |
Completeness [%] | 97.7 | 93.9 |
Redundancy | 4.1 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.1 | 289 | containing 36% 2-Methyl-1,3-Propanediol, 0.1M phosphate-citrate, pH 4.1, VAPOR DIFFUSION, SITTING DROP, temperature 289K |