4M8G
Crystal structure of Se-Met hN33/Tusc3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9787 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 39.107, 64.456, 62.467 |
Unit cell angles | 90.00, 92.45, 90.00 |
Refinement procedure
Resolution | 44.836 - 2.000 |
R-factor | 0.229 |
Rwork | 0.229 |
R-free | 0.24840 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.475 |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.450 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.072 | 0.322 |
Number of reflections | 20996 | |
<I/σ(I)> | 31.1 | 11.4 |
Completeness [%] | 100.0 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 0.2 M KSCN, 10.5% PEG 8K, 10% PEG 1K in 100 mM cacodylic acid-NaOH, pH 6.5, VAPOR DIFFUSION, SITTING DROP |