4M4I
Radiation damage study of Cu T6-insulin - 0.12 MGy
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | Cu FINE FOCUS |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-06-14 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 |
Unit cell lengths | 80.643, 80.643, 33.320 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 16.746 - 1.900 |
R-factor | 0.1673 |
Rwork | 0.165 |
R-free | 0.20160 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.047 |
Data reduction software | CrysalisPro |
Data scaling software | CrysalisPro |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 16.750 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Number of reflections | 6340 | |
Completeness [%] | 99.6 | 99.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 298 | 0.05M sodium citrate, 15%(v/v) acetone, 7.5mM copper(II)acetate, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 298K |