4LY5
Crystal structure of NaASP2 with Zn2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-06-12 |
Detector | RIGAKU RAXIS HTC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 38.100, 51.860, 43.580 |
Unit cell angles | 90.00, 113.88, 90.00 |
Refinement procedure
Resolution | 31.600 - 1.664 |
R-factor | 0.19298 |
Rwork | 0.191 |
R-free | 0.23269 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1u53 |
RMSD bond length | 0.021 |
RMSD bond angle | 2.013 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.600 | 1.690 |
High resolution limit [Å] | 1.660 | 1.660 |
Rmerge | 0.058 | 1.832 |
Number of reflections | 18302 | |
<I/σ(I)> | 13.5 | 0.8 |
Completeness [%] | 99.8 | 96.5 |
Redundancy | 6.4 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 100mM imidazole, 40% PEG 400, 10mM ZnCl2 , pH 8.5, VAPOR DIFFUSION, SITTING DROP |