4LWP
Crystal structure of PRMT6-SAH
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 101.428, 108.465, 137.865 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.596 - 2.353 |
R-factor | 0.2068 |
Rwork | 0.204 |
R-free | 0.24930 |
Structure solution method | SAD |
RMSD bond length | 0.009 |
RMSD bond angle | 1.198 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.350 |
Number of reflections | 31792 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 100 mM Citrate pH 5.5, 20% PEG3000, VAPOR DIFFUSION, HANGING DROP, temperature 293K |