4LTB
Coiled-coil domain of TRIM25
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-02-08 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.669, 83.158, 92.851 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.209 - 2.590 |
R-factor | 0.2082 |
Rwork | 0.203 |
R-free | 0.25720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.165 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX ((AutoMR)) |
Refinement software | PHENIX ((phenix.refine: dev_1427)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 13941 | |
<I/σ(I)> | 17.3 | 2.2 |
Completeness [%] | 96.9 | 81.4 |
Redundancy | 13.1 | 9.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 290 | 6-12% PEG 4000, 10 mM sodium acetate, pH 5.3-6.6, VAPOR DIFFUSION, SITTING DROP, temperature 290K |