4LSF
Ion selectivity of OmpF soaked in 0.1M KBr
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-06-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.91956 |
Spacegroup name | P 3 |
Unit cell lengths | 116.632, 116.632, 51.253 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.158 - 1.900 |
R-factor | 0.2687 |
Rwork | 0.267 |
R-free | 0.29850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2omf |
RMSD bond length | 0.015 |
RMSD bond angle | 1.503 |
Refinement software | PHENIX ((phenix.refine: 1.7.2_869)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.098 | 0.787 |
Number of reflections | 61382 | |
<I/σ(I)> | 20 | 1.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 50% PEG200, 0.1 M sodium cacodylate, 0.2 M magnesium chloride, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K |